Building a true recording-worthy room sucks.
I was unskilled labor in a build of a professional studio towards the end of high school. The studio was located in one suite wihin an office park. Fortunately, the office park was several seperate buildings with several suite per building, each taking the whole space from front to back of the building. So we really only had to worry about the folks on either side.
Anyway, inside the building was setup to be 2 story. The outer structure was cinder block and a corrugated steel roof, with a cement floor. Naturally, each office space was finished out as normal.
First job was to demolish everything inside the space to the cement floor, steel roof and cinder block walls. Then, we had about a hundred cans of expanding foam, and went through filling every crack, crevice and gap in the entire space, much of which was between the roof and the walls. I spent hours upon hours upon hours doing that.
When everything was sealed, fiberglass boards were attached to the cinder block walls, each panel being about 3 inches thick. There were 2 complete layers of those panels, floor to cieling, covering the entire inside of the space.
Next, framing was done, which was attached to the cement floor. This completely framed out the main space, a couple of iso booths and the control room, but was done primarily to give structural support and to attach some of the basic wiring to be done. Within this framework, a second frame was built for each individual room, maybe 8-12 inches seperated from the first framework. Each of these was floated off the cement floor on rubber discs. I know that before the actual subfloor and finsihed flooring were installed for each room that sand was used to fill the dead space, but I'm not positive what they used between the seperate frames. I wasn't there for a good bit of the finish work, cause I didn't already know how to do it.
I can attest that they had bands in there with screaming stacks all hours of the day and night, and never had a single complaint from the business neighbors. They were concerned about that, and also about hearing a firetruck rumbling down the road outside the studio.
I dunno what all was done with HVAC stuff, but I never could detect and a/c related noises at any time in there.